Welcome to the experimental world of Pharmaceutical Analysis. This practical book has been carefully drafted to provide you with a solid foundation in the experimental concepts and basic fundamental in this field. Lab experiments are categorized according to type of titration or technique. Each technique is introduced before experiments. In most of the labs experiments molar and Normal solution are used as followed in recent edition of Indian Pharmacopoeia. Question are presented throughout each experiment. It is important for the students to answer each questions as it will help to improve understanding about experiments. This practical book is the outcome of numerous efforts of authors to incorporate the practical knowledge of Pharmaceutical Analysis. Which has been a requirement of curricula of Pharmacy council of India. This book comprises with 19 Practical’s with short notes as well as viva questions.