Harald Pasch's Books

HPLC of Polymers

By: Harald Pasch,Bernd Trathnigg

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Polymers are mainly characterized by molar mass, chemical composition, functionality and architecture. The determination of the complex structure of polymers by chromatographic and spectroscopic methods is one of the major concerns of polymer analysis and characterization. This lab manual describes the experimental approach to the chromatographic analysis of polymers. Different chromatographic methods, their theoretical background, equipment, experimental procedures and applications are discussed. The book will enable polymer chemists, physicists and material scientists as well as students of macromolecular and analytical science to optimize chromatographic conditions for a specific separation problem. Special emphasis is given to the description of applications for homo- and copolymers and polymer blends.

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Page Count

234

Publisher

Springer Science & Business Media

Published Date

ISBN 10

3642582656

ISBN 13

9783642582653

Advanced Separation Techniques for Polyolefins

By: Harald Pasch,Muhammad Imran Malik

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Advanced Separation Techniques for Polyolefins

By: Harald Pasch,Muhammad Imran Malik

This Springer Laboratory volume introduces the reader to advanced techniques for the separation and fractionation of polyolefins. It includes detailed information on experimental protocols and procedures, addressing the experimental background of different polyolefin fractionation techniques in great detail. The book summarizes important applications in all major fractionation methods with emphasis on multidimensional analytical approaches. It comprises the most powerful modern techniques, such as high temperature size exclusion chromatography (HT-SEC) for molar mass analysis, temperature rising elution fractionation (TREF) and crystallization analysis fractionation (CRYSTAF) for the analysis of chemical composition and branching, high temperature two-dimensional liquid chromatography (HT-2D-LC), solvent and temperature gradient interaction chromatography (SGIC and TGIC) and crystallization elution fractionation (CEF). Beginners as well as experienced chromatographers will benefit from this concise introduction to a great variety in instrumentation, separation procedures and applications. With detailed descriptions of experimental approaches for the analysis of complex polyolefins, the readers are offered a toolbox to solve simple as well as sophisticated separation tasks. The book starts with an introduction into the molecular complexity of polyolefins - the most widely used synthetic polymers with rapidly growing production capacities. It systematically discusses crystallization based fractionation techniques including TREF, CRYSTAF and CEF and column chromatographic techniques for molar mass, chemical composition and microstructure, as well as the combination of different fractionations in multidimensional experimental setups. This book also includes basic information on the application of high-temperature field-flow fractionation.

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Page Count

189

Publisher

Springer

Published Date

ISBN 10

3319086324

ISBN 13

9783319086323

MALDI-TOF Mass Spectrometry of Synthetic Polymers

By: Harald Pasch,Wolfgang Schrepp

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MALDI-TOF Mass Spectrometry of Synthetic Polymers

By: Harald Pasch,Wolfgang Schrepp

MALDI-TOF mass spectrometry is one of the latest and most fascinating new developments in the analysis of organic compounds. Originally developed for the analysis of biomolecules, it has developed into one of the most powerful techniques for the characterization of synthetic polymers. This book describes the fundamentals of the MALDI process and the technical features of MALDI-TOF instrumentation. It reviews the application of MALDI-TOF for identification, chemical and molar mass analysis of synthetic polymers. With many examples, the monograph examines experimental protocols for the determination of endgroups, the analysis of copolymers and additives, and the coupling of liquid chromatography and MALDI-TOF in detail.

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312

Publisher

Springer Science & Business Media

Published Date

ISBN 10

3662050463

ISBN 13

9783662050460

Thermal Field-Flow Fractionation of Polymers

By: Guilaume Greyling,Harald Pasch

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Thermal Field-Flow Fractionation of Polymers

By: Guilaume Greyling,Harald Pasch

This book introduces the reader to thermal field-flow fractionation and discusses its advantages over the fundamental problems associated with traditional column-based analytical techniques commonly used to characterize polymers and macromolecules. The authors discuss the theoretical background, equipment, experimental procedures as well as the recent advances and applications of thermal field-flow fractionation. Complete with several practical examples and troubleshooting guidelines, the book is written for beginners and experienced separation scientists alike and will enable its readers to optimize their experimental conditions for their specific separation needs and problems.

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125

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Springer

Published Date

ISBN 10

3030106500

ISBN 13

9783030106508

Multidimensional HPLC of Polymers

By: Harald Pasch,Bernd Trathnigg

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Multidimensional HPLC of Polymers

By: Harald Pasch,Bernd Trathnigg

This book presents the principle ideas of combining different analytical techniques in multi-dimensional analysis schemes. It reviews the basic principles and instrumentation of multi-dimensional chromatography and the hyphenation of liquid chromatography with selective spectroscopic detectors and presents experimental protocols for the analysis of complex polymers. It is the consequent continuation of "HPLC of Polymers" from 1999 by the same authors. Like its 'predecessor', this book discusses the theoretical background, equipment, experimental procedures and applications for each separation technique, but in contrast treats multi-dimensional and coupled techniques. "Multidimensional HPLC of Polymers" intends to review the state of the art in polymer chromatography and to summarize the developments in the field during the last 15 years. With its tutorial and laboratory manual style it is written for beginners as well as for experienced chromatographers, and will enable its readers (polymer chemists, physicists and material scientists, as well as students of polymer and analytical sciences) to optimize the experimental conditions for their specific separation problems.

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291

Publisher

Springer Science & Business Media

Published Date

ISBN 10

3642360807

ISBN 13

9783642360800

Polymer Synthesis: Theory and Practice

Fundamentals, Methods, Experiments

By: Dietrich Braun,Harald Cherdron,Helmut Ritter

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Polymer Synthesis: Theory and Practice

Fundamentals, Methods, Experiments

By: Dietrich Braun,Harald Cherdron,Helmut Ritter

This Laboratory Manual contains detailed descriptions for the synthesis and characterization of macromolecules. Around 110 elaborated examples, consisting of descriptions of experiments, as well as sufficient theoretical explanations enable the reader to learn about the syntheses, modification, characterization and properties of polymers including recent developments. All experiments can be conducted with adequate laboratory equipment. Suitable for students in organic and polymer chemistry as well as for chemists in industry who want to acquaint themselves with the theoretical and practical aspects of macromolecular chemistry.

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347

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Springer Science & Business Media

Published Date

ISBN 10

3662045737

ISBN 13

9783662045732

Benzodiazepines II

A Handbook. Basic Data, Analytical Methods, Pharmacokinetics, and Comprehensive Literature

By: Harald Schütz

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Benzodiazepines II

A Handbook. Basic Data, Analytical Methods, Pharmacokinetics, and Comprehensive Literature

By: Harald Schütz

... this is an excellent compilation of data which should be on the bookshelves of all analysts interested in the benzodiazepines. It is to be hoped that, with the introduction of so many new ben zodiazepines, the author will quickly add these in a second edi tion" (A. C. Moffat in: Trends in Analytical Chemistry, 1983). This review, deputizing for many others, reflects the friendly reception enjoyed by the first volume of Benzodiazepines, which was published in 1982 and apparently closed a gap in the ben zodiazepine literature. In the meantime, Benzodiazepines has established itself as a standard book, as evidenced by numerous letters and quotations. Suggestions were also soon made for a new edition in view of the unusually rapid development in the field of the benzodiazepines. It became quickly obvious, however, that it would not be sufficient to publish a revised second edition, but that a completely new second volume would be required for which, however, the successful previous format could be largely retained. The following considerations seem worth mentioning in connection with the preparation of Volume II: - To ensure continuity with Volume I as far as possible, the list of references was consecutively numbered (references 1 to 3779 in Volume I, references 3780 to 11338 in Volume II). Whereas in Vol. I the substances appear in the sequential order of their historical development they are listed in alphabetical order in Vol. II.

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Page Count

621

Publisher

Springer Science & Business Media

Published Date

ISBN 10

3642740316

ISBN 13

9783642740312

Thermal Field-Flow Fractionation of Polymers

By: Guilaume Greyling,Harald Pasch

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Thermal Field-Flow Fractionation of Polymers

By: Guilaume Greyling,Harald Pasch

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Page Count

125

Publisher

Springer

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ISBN 10

3030106500

ISBN 13

9783030106508

MALDI-TOF Mass Spectrometry of Synthetic Polymers

By: Harald Pasch,Wolfgang Schrepp

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MALDI-TOF Mass Spectrometry of Synthetic Polymers

By: Harald Pasch,Wolfgang Schrepp

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Page Count

312

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Springer Science & Business Media

Published Date

ISBN 10

3662050463

ISBN 13

9783662050460

Book's by Harald Pasch

HPLC of Polymers

HPLC of Polymers

Advanced Separation Techniques for Polyolefins

Advanced Separation Techniques for Polyolefins

MALDI-TOF Mass Spectrometry of Synthetic Polymers

MALDI-TOF Mass Spectrometry of Synthetic Polymers

Thermal Field-Flow Fractionation of Polymers

Thermal Field-Flow Fractionation of Polymers

Multidimensional HPLC of Polymers

Multidimensional HPLC of Polymers

Polymer Synthesis: Theory and Practice

Polymer Synthesis: Theory and Practice

Benzodiazepines II

Benzodiazepines II

Thermal Field-Flow Fractionation of Polymers

Thermal Field-Flow Fractionation of Polymers

MALDI-TOF Mass Spectrometry of Synthetic Polymers

MALDI-TOF Mass Spectrometry of Synthetic Polymers

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